Hellow,

I analysed trimethyl borate on GC capillary column [CPSiL-5CB] I got the peak but one additional peak which is just near about the main peak is continuous vary with run to run . I also got this peak and it is methanol peak , but i still not understand how can I catch repeatibility for the analysis . should I change the Gc column or can any one suggest me the apropriate method of analysis of Trimethyl borate

Thanks in advance

praveen
email paliwalpraveen@yahoo.co.in