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How to check the TCD detector broken or not?

Discussions about GC and other "gas phase" separation techniques.

5 posts Page 1 of 1
I tried measure the resistance and I can hear the clicking sound. Is there any other way to check?
Thanks!
Do you get a signal when you run a standard?
----suffers separation anxiety----
Hi,

Thanks for your response and help.
When I turn on the TCD detector, the signal turn from straight line to noise. When I increase the mass flow rate from 18 to 25, the noise position changed from about 0.1 to 0.2. I don't have standard gas, I just use 2 percent oxygen in Ar. There is no peak. I used 2 percent C3H6 in Ar, still no peak.

Another question, will the reference and make up gas flow rate affect a lot? I just wanna see a peak.

Thanks!
How are you introducing your sample gas to the GC?
----suffers separation anxiety----
Six way valve, this valve works since I used it for FID detector and there is peak.thanks!
5 posts Page 1 of 1

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