Advertisement

Help! I got water in my SS lines...

Discussions about GC and other "gas phase" separation techniques.

4 posts Page 1 of 1
Has anybody had success purging water from their SS GC lines? A fault in a H2 generator caused water to enter my lines and I don't want to spend money to replace them. I only have about 20 total feet of tubing, so I was thinking of just hooking up a N2 cylinder and running that at high pressure for a few days.

Any ideas or experience in a similar situation is very much appreciated!
What is the cost of nitrogen compared to the cost of new pipes is question one.

If the pipes are at room temperature it will take forever to dry them out - is there any way that you can heat them up with a hot air gun or even a hair dryer, starting at the cylinder end ?

Peter
Peter Apps
If you purge the line with N2 at high pressure and for a few days , you will pay more for N2 than the tubing .

Try washing the tubing with methanol or IPA first , may be using a 50 ml syringe , then purge with N2 for a few minutes.

Take care to avoid fire hazard during the procedure.
I clean tubing by dripping acetone down them and then throwing them in an oven for 125degC overnight.
4 posts Page 1 of 1

Who is online

In total there are 58 users online :: 1 registered, 0 hidden and 57 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: Majestic-12 [Bot] and 57 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry