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Spectral scan issues
Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.
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Spectral scan is a blob from mass 50 to around 500 after changing column and cleaning source. Any suggestions?
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what kind of instrument? GC/MS? LC/MS? Make and Model would help as well.
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HP GC/MS 5973. Changed to new source, changed EM, isolated column, looked for backstreaming of diffusion oil, loaded old tune thinking it may be a corrupt tune issue. Doesnt seem to be any of these. Gonna change HED and source assembly next. Any ideas would be appreciated.
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Any history on this? Did this happen all at once or has this progressed over time? And how do the quads look?
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It happened all at once. I have actually took the whole sideplate with quads and installed it on another instrument and it worked fine.
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My thougths go in the direction of an electronics failure - given that you describe some kind of signal, but badly formed, perhaps something related to the radio frequency generator for the quads. (And that perhaps is a guess. It has been so long ago that I had an RF section go out - and I think that was on a 5972, the symptoms are far back and lost in history for me.)
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