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Spectral scan issues

Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.

6 posts Page 1 of 1
Spectral scan is a blob from mass 50 to around 500 after changing column and cleaning source. Any suggestions?
what kind of instrument? GC/MS? LC/MS? Make and Model would help as well.
HP GC/MS 5973. Changed to new source, changed EM, isolated column, looked for backstreaming of diffusion oil, loaded old tune thinking it may be a corrupt tune issue. Doesnt seem to be any of these. Gonna change HED and source assembly next. Any ideas would be appreciated.
Any history on this? Did this happen all at once or has this progressed over time? And how do the quads look?
It happened all at once. I have actually took the whole sideplate with quads and installed it on another instrument and it worked fine.
My thougths go in the direction of an electronics failure - given that you describe some kind of signal, but badly formed, perhaps something related to the radio frequency generator for the quads. (And that perhaps is a guess. It has been so long ago that I had an RF section go out - and I think that was on a 5972, the symptoms are far back and lost in history for me.)
6 posts Page 1 of 1

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