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Toxaphene analysis by Thermo Finnigan MAT95 HR/GCMS NCI

Posted: Thu Jul 12, 2012 5:33 pm
by tolo
I am going to work in Toxaphene analysis using Thermo Finnigan Mat95 HR/GCMS NCI mode (Reagent Gas : Methane)

Anybody knows how to perform the mass tuning in HR in NCI mode? I just know the procedure for EI/HRGCMS.

Question?

1. Initial check for NCI / Methane reagent / leak .........
2. Mass calibration for resolution 10000
3. Set up the MID table

Re: Toxaphene analysis by Thermo Finnigan MAT95 HR/GCMS NCI

Posted: Thu Jul 26, 2012 12:17 pm
by Bigbear
I do Toxaphene and chlordane in water via EPA 525. I set up a sim method and I tune to DFTTP.