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- Posts: 14
- Joined: Thu Apr 28, 2011 7:50 am
I woul like here to expose some problems with the Teledyne Tekmar Atomx. Frequently the standard addition is not succesfull. The process that i go on is: After initialize the syringe and leak check, and prime with water and methanol... first: Tools/prime change standard then open the vessels and fill them. Afterwards: Tools/check standard pressure and follow the procedure indicatedd on screen. Finally: Tools/Prime Change Standard x or all standards. Sometimes i repeat the process x times and then get the goal, but it is very time consuming and standard consuming since the volume vessel is effectivily reduced without mixing with the sample?¿?¿!!!
Otherwise, perhaps related, when i pressurize the system : Tools/check standard pressure, the pressure rise very fast and even is difficult to set the require value ( 7.0 psig) pushing STEP when is achieved. The firsts times i did that process, the pressure rise more slowly. Apparently nothing has changed to.
Thank in advance,
Ricard
