Fronting peaks in GC
Posted: Thu May 12, 2005 12:56 pm
The analyte I'm interested in fronts quite badly.
The compond is a primary amine and I'm running on an RTX amine phase.
Loading seems OK for the column I'm using (30m x .32 x 0.5u) and I think I've got correct flows etc.
Any ideas whats causing this and any tips to try and avoid it ?
TIA
Stanlee
The compond is a primary amine and I'm running on an RTX amine phase.
Loading seems OK for the column I'm using (30m x .32 x 0.5u) and I think I've got correct flows etc.
Any ideas whats causing this and any tips to try and avoid it ?
TIA
Stanlee