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Resolution of Bis(2-Chloroethyl)ether and Aniline

http://www.chromforum.org/viewtopic.php?t=18834

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Resolution of Bis(2-Chloroethyl)ether and Aniline

Posted: Thu Jan 19, 2012 10:01 pm
by a2j812
Can anyone help me get resolution between Bis(2-Chloroethyl)ether and Aniline?

Re: Resolution of Bis(2-Chloroethyl)ether and Aniline

Posted: Tue Jan 24, 2012 12:34 am
by mckrause
Yeah, it's not great. We get baseline (barely), using a 20 m x 0.18 mm 0.18 um Restek RXi-5Sil-MS, starting at 50 C. It's tricky - you need to balance your gas flows well, so that you're at optimum flow throughout the front part of the chromatogram.
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