-
- Posts: 22
- Joined: Tue Jul 05, 2011 9:59 am
Advertisement
IS 105% recovery acceptable
Discussions about sample preparation: extraction, cleanup, derivatization, etc.
3 posts
Page 1 of 1
I am extracting an analyte from a polymer emulsion by precipitaiing the polymers along with water. I am getting a recovery of 106%,105% and 104% at 1st 2nd and 3rd level.The average recovery is 105%. Is this ok or shall I consider changing the extraction method.My boss really does not want to change the method because of the time and cost we have done already for this method.
-
- Posts: 3594
- Joined: Mon Aug 30, 2004 11:43 pm
Food and Drug Administration, ORA Laboratory Procedure ORA-LAB.5.4.5, version 12, revised 9-9-2005, including Appendix I, gives a range of 95-105% recovery acceptable for spiked samples.
-
- Posts: 22
- Joined: Tue Jul 05, 2011 9:59 am
Thank you for Consumer Products Guy
3 posts
Page 1 of 1
Who is online
In total there are 10 users online :: 0 registered, 0 hidden and 10 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am
Users browsing this forum: No registered users and 10 guests
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am
Users browsing this forum: No registered users and 10 guests
Latest Blog Posts from Separation Science
Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.
Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.
- Follow us on Twitter: @Sep_Science
- Follow us on Linkedin: Separation Science
