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co/co2 problem in co/co2 analyzer

Posted: Sat Apr 09, 2011 5:55 am
by mr3573
Recently I changed the catalyst tube for co/co2 analyzer. I used the packed tube that means we purchased packed tube and not fill by ourselves. Now I have problem with both CO and CO2 as shown I attached file. How could adjust GC condition to obtain linear base line and symmetrical peak for both

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Re: co/co2 problem in co/co2 analyzer

Posted: Sat Apr 09, 2011 12:59 pm
by chromatographer1
You should not have to change conditions if you purchased a replacement catalyst tube from your supplier.

The problem is with your tube, not the GC conditions. It does not appear to be working properly.

I recommend you call the vendor, explain the results and get a new tube.

Re: co/co2 problem in co/co2 analyzer

Posted: Tue Apr 12, 2011 11:15 am
by sheikh1299
i have a ploblemes with Gc-3800
CO/CO2 by FID
extra peak in area temprather programing ?
please help me