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- Posts: 6
- Joined: Tue Sep 21, 2010 7:56 pm
The negative dip occurs at the tail of most of the analytes we are separating (not SO42-, perhaps because it is a broad peak?). We only integrate for Cl- and SO42- and it is interfering with our Cl- calibration curve. The problem persists in all of our standards/ working samples and gets more pronounced with higher concentrations. Our working samples consist of Denatured Fuel Ethanol (no dilution) and Antifreeze (100:1 dilution). At this point we have tried everything that we can think of and are at a complete loss.
Any suggestions? Thanks!














 
																							