-
- Posts: 2
- Joined: Sun Dec 21, 2008 3:58 am
Advertisement
MSD5973 oil contamination problem
Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.
3 posts
Page 1 of 1
In a moment of insanity under too much work stress, I did a major mistake opening MSD (GC6980/MSD5973) without proper venting and cooling… Immediately saw the “smokeâ€
-
- Posts: 176
- Joined: Mon Mar 14, 2005 7:01 pm
Hello
Habitually, the oil trace will disappears with time.....you can increase the temperature of your source and the quad for help you.
Habitually, the oil trace will disappears with time.....you can increase the temperature of your source and the quad for help you.
-
- Posts: 1680
- Joined: Sat Aug 23, 2008 12:04 am
This brings back memories - and it's been a while ago, so it may have been a 5972 rather than a 5973 that backstreamed on us. We pulled the analyzer section, removed the source and detector and washed the quads down by pouring methylene chloride through them. We replaced the detector and cleaned the source. The instrument showed a high background for methylene chloride for a few days, but it recovered and ran quite well after that. Just be careful, the 5972 had machined quad rods. The 5973 has the metal film on quartz - and it may not take much abuse. But if it is oil coated, there may not be much to lose...
Good luck.
Good luck.
3 posts
Page 1 of 1
Who is online
In total there are 32 users online :: 0 registered, 0 hidden and 32 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am
Users browsing this forum: No registered users and 32 guests
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am
Users browsing this forum: No registered users and 32 guests
Latest Blog Posts from Separation Science
Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.
Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.
- Follow us on Twitter: @Sep_Science
- Follow us on Linkedin: Separation Science
