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alkyl mesylates in Pharmaceutical formulation

Posted: Wed Jun 04, 2008 12:42 am
by dcobice
Hi all,
Im a dealing with mesylates by GC/MS/SIR with SPE and Liquid/liquid microextraction and I couldnt ahieve good recovery.
any suggestion, tecniques?? diferents platforms?? derivatization?
Someone has experience with tiocyanate derivatization using HS/GC/MS/SIR??

thanks in advance!

diego