Loss of sensitivity on GC/MSD
Posted: Thu Feb 07, 2008 12:46 pm
I work at a GC/MSD (6890/5973).
The system was low sensitivity, as far as sometimes that didn't has response: the chromatogram didn't has peak and the autotune was horrible.
I cleaned the ion source and the system worked better: the autotune was goog, although the sensitivity wasn't the same of before (when the system was OK). But after to perform some injections the problem returned.
¿What can the problem be?
The system was low sensitivity, as far as sometimes that didn't has response: the chromatogram didn't has peak and the autotune was horrible.
I cleaned the ion source and the system worked better: the autotune was goog, although the sensitivity wasn't the same of before (when the system was OK). But after to perform some injections the problem returned.
¿What can the problem be?