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Garlic

Discussions about HPLC, CE, TLC, SFC, and other "liquid phase" separation techniques.

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I am trying to determine the Allicin content of garlic powder by HPLC (european pharmacopoiea). There are quite a few peaks present and the monograph does not help identify the allicin peak. Does anyone have an example chromatogram or know of the retention time relative to the internal standard.

Thanks

This reference gives an example chromatogram - hope it is helpful.

http://jn.nutrition.org/cgi/content/full/131/3/968S
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