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Using A Gas Chromatograph

Posted: Thu Sep 09, 2004 7:58 pm
by WTG2002
Hi, my name is Travis Garrett. I am currently working on a BS in Chemistry and am taking Instrumental Analysis. As part of the lab, we are assigned an instrument and we are supposed to do a report, learn to use the instrument and conduct an experiment for to teach the class with under the supervision of the instructor. I was wondering if anyone here had worked with a GOW-MAC Series 350 Gas Chromatograph with a TCD? I am just reading through the manual and reading some books about gas chromatography in general. Any help all you of you can give me would be greatly appreciated.

Travis

Posted: Thu Sep 09, 2004 11:24 pm
by tom jupille
There is also a wealth of information on-line (for example:
http://ull.chemistry.uakron.edu/chemsep/gc/ )

You've probably already done this, but a Google search on "gas chromatography" will return a wealth of information.

As to specific class experiments, what you can do will depend a lot on what column(s) the instructor has available for your instrument. As you've probably already discovered, a GC is a very general instrument. It must be adapted to a specific analysis by choosing an appropriate column ("stationary phase").

Aside from that, the only real requirement is that your sample be volatile and/or thermally stable. Some possibilities:
  • - the amount of CO2 in exhaled breath
    - hydrocarbon distribution in lighter fluid
    - alcohol in a dry martini
    - antifreeze (ethylene glycol) in water
Any of these are straightforward if you have an appropriate column.

How elaborate you want to get depends on the goals of the class:
  • - do you want everyone to make an injection (sort of "show and tell")?
    - do you want to work in teams and go through quantitation (injecting standards, generating a calibration plot, and then quantitating a "sample")?
    - do you want to explore the chromatographic process (e.g., effect of carrier gas flow rate on peak width?)
Once you have that aspect (how elaborate) defined, come back and post again for some specific suggestions from practitioners.

Posted: Fri Oct 29, 2004 1:28 am
by chemist
Tom can you give me more basic info on GC for my science fair project. I'm really doing paper chromatography, but for the fair I need to define what the other ones are and the difference between them and the one i'm doing. Any info would be greatly appreciated.

Posted: Fri Oct 29, 2004 8:01 pm
by Davide
Hello, what you to do with your GC TCD ? this will be helpfull if you say what are your question(s) about chromatography.

Posted: Sun Oct 31, 2004 10:09 pm
by chemist
I'm doing a projecty about paper chromatography and I need basic, what is it, what does it do, and why does do this information. Do you now where I can get this info on the web??