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H2O2 analysis

http://www.chromforum.org/viewtopic.php?t=7166

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H2O2 analysis

Posted: Tue Oct 23, 2007 1:09 pm
by Chandresh K. Soni
Hi
My Problem is to Analyse the H2O2 Content in a Solid Comp. on GC
Is it possible on FID or on TCD . If yes Then Which Column i Preffered.
pls suggest me.

Posted: Tue Oct 23, 2007 4:31 pm
by MikeD
Not possible by FID and while I would never say never to GC-TCD this article below describes a few HPLC options involving oxidation of substances like triphenylphosphine or formation of iron (III) or titanium (IV) complexes.

http://www.rsc.org/delivery/_ArticleLin ... i=a806432f
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