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Analysing Organochlorines pesticides in leek

Posted: Wed Sep 08, 2004 2:55 pm
by UMAchem
Hi to all!
How to prepare the leek sample for analyse in a GC-ECD?
We use GPC for cleanup, but we only can see peaks under Rt= 20 minutes. The time before that RT, we only see a large band. That method with other commoditys give good results.

Any sugestion?

Thanks for your help in advance!