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Haloacetic acid analysis

Posted: Tue Sep 07, 2004 6:57 pm
by organicdude
Does anybody in here run EPA 552.2? I've been having a problem with internal standard recovery (1,2,3-trichloropropane). There seems to be some inconsistency in some of the samples. Are you familiar with any interferences that would affect an inconsistent internal standard recovery?(calculated by area). I haven't experienced this before.

I've looked at some of the newsgroups on Google, and couldn't find anything; I haven't found anything in the method either (hopefully I didn't skim right past it.)

Any suggestions would be appreciated. Thanks.