From Packed to Capillary
Posted: Thu Aug 30, 2007 2:17 pm
I am trying to peform the related substances of Tranylcypromine Sulphate. The BP method says to use the following column:
- Glass column (1.5 m × 4 mm) packed with acid-washed, silanised diatomaceous support (100 to 120 mesh) coated with 3% w/w of cyanopropylmethylphenyl methyl silicone fluid (OV-225 is suitable).
Does anyone know of any capillary columns that could be used as an alternative or which suppliers in the UK still offer a wide range of packed columns.
Thanks
- Glass column (1.5 m × 4 mm) packed with acid-washed, silanised diatomaceous support (100 to 120 mesh) coated with 3% w/w of cyanopropylmethylphenyl methyl silicone fluid (OV-225 is suitable).
Does anyone know of any capillary columns that could be used as an alternative or which suppliers in the UK still offer a wide range of packed columns.
Thanks