Advertisement

Calibrating group peaks

Discussions about GC and other "gas phase" separation techniques.

3 posts Page 1 of 1
I have an analyte with four peaks (Dipropylene glycol). The calibrated amount is reporting as a different amount for each peak instead of the group. How can I correct?

Use your integration software to sum the four peaks and report it as one peak.

Not knowing if you have any other peaks within the time span of the four or what brand of software you have (if it isn't the same as mine I cannot help you) there is not much else to say.

Good luck,

Rod

Here we do as Rod states, use summation and then have "one peak" for the datastation to easy use for calibration. This is especially useful if your DPG standard is from a different lot or supplier, as the peak ratios vary. Most times we trimethlsilylate the DPG and use nonpolar capillary, but have done "as-is" on polar capillary too.
3 posts Page 1 of 1

Who is online

In total there are 46 users online :: 0 registered, 0 hidden and 46 guests (based on users active over the past 5 minutes)
Most users ever online was 5108 on Wed Nov 05, 2025 8:51 pm

Users browsing this forum: No registered users and 46 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry