HELP WANTED !(Varian CP 3800)

[bublle]

I have problems in establishing split ratio-splitting wanted relation.
At first I've menaged to have splitting measured with flowmeter around 40 ml/min when the split ratio set in the method was 40.
Nowadays at split ratio 40 I have value around 129-135 ml/min on the flowmeter.
What could be the cose?Why don't they follow each other?
Septum,column and detector are checked!
How to establish splliting arond 40 when I have set in the method split ratio at 40?????
Could possibly water in H2 geneartor that has lager concentration of co2 have influence?

Thank you!!!!!

[Peter Apps]

The split ratio is the ratio of the flow out of the split to the flow into the column. Only if the flow into the column is 1 ml/min will the split flow be 40 ml/min at a split ratio of 40:1. At higher flows into the column the split flow will be higher for the same split ratio.

Peter

[bublle]

Hi Peter!
Just want to thank you for the explanation.
Mail ya.