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Electron Capture Detector

Posted: Sat Sep 30, 2006 2:01 am
by Ashraf_Khan
What causes negative peaks or negative humps in a GC-ECD, even in a dry run (no injection), an air injection or in a blank solvent (hydrocarbon) injection ? What are the remedies for these random and/or non-random phenomena?

Thanks.

Posted: Sat Sep 30, 2006 4:08 am
by ntruong
Hi,
There could be a gas leak in the system.

Posted: Mon Oct 02, 2006 2:30 pm
by L4br4t
Hmmmmm....most likely NOT a leak....but sounds like a dirty cell..have it cleaned or replaced.