GC method for Boc Anhydride (di-tert-butyldicarbonate)
Posted: Fri Sep 22, 2006 9:18 pm
by xxiong
I need a GC method to analyze Boc Anhydride.
It's from Aldrich (#34659).
They analyze it with GC.
Any body has experience for this compound (quantitation)?
Thanks very much.
Xiaobing
xiaobing_xiong@yahoo.com
u can try this
Posted: Wed Sep 27, 2006 11:37 am
by dhruvil
hi, dear
yes i have done this sample
u can use AT-5 ( 30 x 0.53 x 5 um) column and normal oven termperture progamming...
i have analysed this material by liquid injection method on shimadzu GC-14B. where split adjusted was 50:1.
keep your inj/det. temperature to 220/280 C.
ok then hope this will solve your problem..dear
just try thid and reply me what happened,
cu soon
bye
regards
Dhruvil
Posted: Wed Sep 27, 2006 11:57 am
by sadsal123
Dhruvil,
What is ur definition of 'normal oven temperature programming?' Experience tells me that program depends on lots of things: column, carrier gas, analytes, etc, etc.....
