GC method for Boc Anhydride (di-tert-butyldicarbonate)

[xxiong]

I need a GC method to analyze Boc Anhydride.
It's from Aldrich (#34659).
They analyze it with GC.
Any body has experience for this compound (quantitation)?
Thanks very much.
Xiaobing
xiaobing_xiong@yahoo.com

[dhruvil]

hi, dear
yes i have done this sample
u can use AT-5 ( 30 x 0.53 x 5 um) column and normal oven termperture progamming...
i have analysed this material by liquid injection method on shimadzu GC-14B. where split adjusted was 50:1.
keep your inj/det. temperature to 220/280 C.

ok then hope this will solve your problem..dear
just try thid and reply me what happened,

cu soon
bye

regards
Dhruvil

[sadsal123]

Dhruvil,

What is ur definition of 'normal oven temperature programming?' Experience tells me that program depends on lots of things: column, carrier gas, analytes, etc, etc.....