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Analysis of Acetamiprid in vegetable oil

http://www.chromforum.org/viewtopic.php?t=3929

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Analysis of Acetamiprid in vegetable oil

Posted: Thu May 04, 2006 1:27 pm
by along
Dear all.

Did anyone of you analysed before acetamiprid (Insecticide) in vegetable oil matrix....I am currently looking for method to analyse this compound with HPLC, kindly provide your HPLC method if any. Thanks and best regards.

Posted: Thu May 04, 2006 2:53 pm
by Bryan Evans
We have 2 methods using our Cadenza CD C18 column.
The first one is isocratic - the 2nd one is a gradient.
Let me know if we can further assist you - thank you.

http://www.imtakt.com/TecInfo/TI231E.pdf
http://www.imtakt.com/TecInfo/TI230E.pdf

Posted: Thu May 04, 2006 10:57 pm
by Uwe Neue
Out of vegetable oil...

I suggest SPE with a silica sorbent and extraction with methanol or methanol/water after washing out the oil with something like MeCl2.
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