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Method of analysis for methyl methanesulfonate-reg

http://www.chromforum.org/viewtopic.php?t=3681

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Method of analysis for methyl methanesulfonate-reg

Posted: Fri Mar 24, 2006 10:39 am
by sivatorrent
Dear All,

We are searching for a method of analysis of methyl methanesulfonate
(alkyl ester of Methane sulfonic acid) by GC, GC-MS, NMR or else.

Can any one help us by giving some references or method of analysis.

Thanks and Regards,

B.Sivakumar

Methylmethanesulfonate

Posted: Sat Mar 25, 2006 3:32 am
by ddostie
I've used GC/MS to identify Isopropylmethanesulfonate in a reaction mixture using a DB-1 30m x 0.32 x 1um. I would expect the methyl ester to behave analogously. GC/FID would be fine as well, as I only use the MS because I didn't know what it was.

Duane
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