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optimization of flow rate

Posted: Thu Dec 29, 2005 9:31 am
by nina
Hi
I use a CHROMATOPAC for recording peaks in GC/FID.
how can I measure the W1/2 for calculating the effeciency?
I think that accuracy is very low.
thanks
happy new year
nina

Posted: Thu Dec 29, 2005 10:02 am
by Srinivas SK
Hello :D

Are you using CR8A? If so, what's the chart speed?

chart speed

Posted: Mon Jan 02, 2006 1:08 pm
by nina
Hi
I use C-R 6A chromatopac.
chart speed is 5.
happy new year
thanks

Posted: Mon Jan 02, 2006 1:55 pm
by Srinivas SK
Hello:

If you're trying to calculate the plate count manually using CR6A, I'd suggest you take a printout of your chromatogram using a lower chart speed, say, 1 mm/min and use the lowest attentuation possible ( this will be the G key on the CR6A keyboard, the M key is for the chart speed)

You'll get large peaks in the chromatogram printout. This will make it easier for you to choose a peak and directly measure its W1/2 and calculate the plate count from that.

I hope this answers your question.

:D

thank you

Posted: Wed Jan 04, 2006 12:49 pm
by nina
thank you very much.
best regards