amino acids by gc
Posted: Tue Dec 20, 2005 2:28 pm
hi,
amino acid by gc.
any suggestions.
vijay
amino acid by gc.
any suggestions.
vijay
www.phenomenex.com
EZ:faast AA analysis kit, available for GC-FID, GC-MS and LC-MS.
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amino acids by gc
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Posted: Tue Dec 20, 2005 3:11 pm
Posted: Wed Dec 21, 2005 3:38 am
Silyl derivatisation, followed by FID or Ion selective MS, depending on the sample matrix and sample concentration.
If it's a biological matrix, like serum, there will be considerable sample prep to be done.
rgds,
S.K. Srinivas
If it's a biological matrix, like serum, there will be considerable sample prep to be done.
rgds,
S.K. Srinivas
ez faast AA kit
Posted: Fri Dec 23, 2005 11:47 am
Hi all,
I am trying to set up a method using ez faast Protein Hydrolysate kit. Sample preparation variations are much higher than I expected.
When I test Pickering aa reference standarts (each AA 250nmol/ml) after fresh calibration I found that results are varying, ie, some are around 200, some 125.
I don't have much time for troubleshooting until next year
.
Any similar experience?
Happy new year to all.
Foren
I am trying to set up a method using ez faast Protein Hydrolysate kit. Sample preparation variations are much higher than I expected.
When I test Pickering aa reference standarts (each AA 250nmol/ml) after fresh calibration I found that results are varying, ie, some are around 200, some 125.
I don't have much time for troubleshooting until next year
. Any similar experience?
Happy new year to all.
Foren