Advertisement

FPD troubleshooting

Discussions about GC and other "gas phase" separation techniques.

3 posts Page 1 of 1
I am new to FPD and am trying to do some troubleshooting. What could cause almost complete absense of peaks? What is the correct or recomended insertion distance of a capillary column into an HP5890 FPD? My manual recomends 155mm from the end of the column nut, is this correct? There is definitely column flow and the flows at the detector are at their recomended values: 100mL/min for air and 75mL/min for H2. I have tried increasing the amount of H2 gradually to the same as the air with no luck. I have confirmed that the injection is working by switching to the FID I also have installed on this GC. I believe I can detect the solvent on the injection, but my test mix is not showing up at all. Any thoughts?

:D
Your parameters for FPD are good.
You say that you see all the peaks you need with FID,therefore the chromatography works...

:idea: Don't forget to light on your FPD!
:idea: Do you have the right Filter S or P for the right substance?

Tell us a little more about your method....

Bye

The FPD is definitely lit. I have the phosphorus filter in and am running organophosphate pesticides.

Can the filter be a problem? is that something I should need to clean? I just got this detector used, and it may need some more upkeep.
3 posts Page 1 of 1

Who is online

In total there are 18 users online :: 1 registered, 0 hidden and 17 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: Google Adsense [Bot] and 17 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry