GCMS no peaks before 2 minutes
Posted: Mon Nov 03, 2014 6:20 pm
Hi I have a 6890N/5973N GC/MS. For some reason when we run a sample we cannot see any peaks before 2 minutes in the run. After 2 minutes all is fine. The MS is on and the EM has voltage applied. We have the solvent delay turned off (set at 0). The baseline is completely flat prior to the 2 minutes. It looks like the analyzer is not on (but we have EM voltage). Also at exactly the 2 minute mark we hear a click, like something turned on (the MS). Please help.