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Transferring Loop injection to Syringe injection with split

http://www.chromforum.org/viewtopic.php?t=25789

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Transferring Loop injection to Syringe injection with split

Posted: Sat Oct 25, 2014 6:42 pm
by Raphael Divekar
I have a vendor's GC headspace method for determination of impurities and have to adopt in my laboratory. The method uses a loop injection method while we a syringe injection method with a split mode option. How do I set the parameters to achieve the identical sensitivity, precision and accuracy?

Re: Transferring Loop injection to Syringe injection with sp

Posted: Mon Oct 27, 2014 8:55 am
by CE Instruments
It is completely impossible to get IDENTICAL sensitivity, precision and accuracy.
Start by calculating the actual volume transferred and match the incubation conditions and start from there.
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