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- Posts: 13
- Joined: Thu Jun 19, 2014 12:59 am
When power returned it pumped down almost instantly. After auto tuning I did the air and water check and system evaluation.
The system evaluation was ok except "Mass 502 Precursor (<= 12%)" and the value recorded was 16.00
The message "Contact your Agilent Technologies Customer Engineer" appeared underneath that line. I contacted them by the way and they didn't know the cause and said it probably wouldn't affect our analysis anyway. There was also the message "One or more specifications was out of range. Please correct before continuing."
After changing to a method with a higher flow rate and less vacuum (which is more consistent with previous autotunes) I did the tune again and the system evaluation. The Mass 502 value now changed to 13.82, so it appears that it's dropping. Any advice on what I should do (or not do)? Any ideas how the power outage is related to the sudden high abundance of 502?
Also on a tune I did exactly one month ago I noticed the 502 peak start to develop a small hump on the left side at roughly 2.5x the height of the small peak to the right of the main peak. After the power outage after an autotune and spectra tune the hump got a little smoother. After an autotune this morning it got a lot 'sharper' so that it has formed a tiny small peak with no tail connected to the large peak. How can I make it go smooth again so there is no split peak?
