-
- Posts: 1
- Joined: Tue Jul 01, 2014 1:41 pm
Advertisement
Dropping baseline during oven ramp
Discussions about GC and other "gas phase" separation techniques.
5 posts
Page 1 of 1
I operate a Agilent GC-FID 7890B. The baseline recently has just rise to over 100. I have just replaced the jet of the FID detector but the problems still remain. Now normally at 120C oven temperature my baseline after 2-3 hours bakeout is still around 150, but during runs my baseline will suddenly drop gradually even the oven temperature is increasing. The baseline looks like going down stairs. Any suggestions on where the problem originate from? Carrier gas is hydrogen, without other markup gas, and compressed air from an air compressor. Peaks look fine, separation is good just the baseline is horrible. There is a big sliver universal gas trap before the GC.
-
- Posts: 927
- Joined: Mon Feb 13, 2006 6:28 pm
Remove FID insulation inside the oven and retight adapter nut.
-
- Posts: 1680
- Joined: Sat Aug 23, 2008 12:04 am
Be sure you have no leaks around the inlet. If a leak opens with increasing oven temperature, flow thorugh the column will drop.
-
- Posts: 1773
- Joined: Fri Feb 09, 2007 10:33 pm
calvin.poh,
If it were me, I would replace the split vent line and the trap. Odd, but I used to see this on the 5890's.
Best regards,
AICMM
If it were me, I would replace the split vent line and the trap. Odd, but I used to see this on the 5890's.
Best regards,
AICMM
-
- Posts: 927
- Joined: Mon Feb 13, 2006 6:28 pm
IMHO he/she is no longer interested in any advise. If after 10 days we have no feedback ...
5 posts
Page 1 of 1
Who is online
In total there are 130 users online :: 0 registered, 0 hidden and 130 guests (based on users active over the past 5 minutes)
Most users ever online was 5108 on Wed Nov 05, 2025 8:51 pm
Users browsing this forum: No registered users and 130 guests
Most users ever online was 5108 on Wed Nov 05, 2025 8:51 pm
Users browsing this forum: No registered users and 130 guests
Latest Blog Posts from Separation Science
Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.
Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.
- Follow us on Twitter: @Sep_Science
- Follow us on Linkedin: Separation Science
