Chlorine Gas Analysis
Posted: Wed Jun 18, 2014 5:04 pm
I am wondering if anyone has analyzed organic chlorides in dry chlorine gas.
I need to see ppm levels to percent levels for the organic chloride, I am using an FID. So far during column testing I have not been able to find a column that does not react with chlorine, most of the columns seem to have their phase stripped and I get large rolls or phase peaks. The columns I have found that do not react have issues with separation between methyl chloride and chlorine so I can't cut the chlorine to vent.
I need to see ppm levels to percent levels for the organic chloride, I am using an FID. So far during column testing I have not been able to find a column that does not react with chlorine, most of the columns seem to have their phase stripped and I get large rolls or phase peaks. The columns I have found that do not react have issues with separation between methyl chloride and chlorine so I can't cut the chlorine to vent.