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Analytical method for Sodium borohydride content

http://www.chromforum.org/viewtopic.php?t=24766

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Analytical method for Sodium borohydride content

Posted: Fri May 09, 2014 11:11 am
by dhanireddy1982
Dear all,

Can any one provide the method for the determination of Sodium borohydride content by HPLC/GC.

Thanks in advance.

Re: Analytical method for Sodium borohydride content

Posted: Fri May 09, 2014 1:27 pm
by Gerhard Kratz
Direct Volumetric Assay of Sodium Borohydride and Potassium Borohydride
PDF [275 KB]First Page Add to ACS ChemWorx
S. W. Chaikin

Anal. Chem., 1953, 25 (5), pp 831–832
DOI: 10.1021/ac60077a054
Publication Date: May 1953

Maybe ion chromatography will help, it is so reactive, even solved in acetic acid. Good luck.
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