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Building a thermal conductivity detector

Posted: Mon Dec 30, 2013 8:31 pm
by osp001
I found an old DIY paper on the subject (A Simple-to-Build Thermal-Conductivity GC Detector, from J. Chem Ed in 1994), but I was hoping for a rather more sensitive detection method. That paper uses a 1N914 signal diode, while I'd prefer to make one using rhenium/tungsten wire for sensitivity purposes.

Anyone ever go about this? I'd be interested in details.

Re: Building a thermal conductivity detector

Posted: Tue Feb 25, 2014 12:03 am
by AICMM
osp001,

What do you want to measure? How hot? Look at thermistors. Small, very sensitive but only at low temperatures and NO, NO to hydrogen.

Be aware that tungsten/rhenium versions are highly coiled to get sufficient resistance to get decent current drop.

Best regards,

AICMM