Advertisement

temperature settings 5973

Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.

5 posts Page 1 of 1
I vented the system last week and cleaned the source, during pump down the temperature (actual) reading for the source heater was bouncing around between 170-500 degrees (set at 230) and the quadrupole never reached the set temperature of 150 (stayed around 80). I was told main board or side board by agilent. Any ideas or suggestions in case its something I can try to reset. I have already redone the pump down after opening the system back up and checking connections and changed out the heater source assembly.
I vented the system last week and cleaned the source, during pump down the temperature (actual) reading for the source heater was bouncing around between 170-500 degrees (set at 230) and the quadrupole never reached the set temperature of 150 (stayed around 80). I was told main board or side board by agilent. Any ideas or suggestions in case its something I can try to reset. I have already redone the pump down after opening the system back up and checking connections and changed out the heater source assembly.
If the heaters are new replacements, then remove the covers on the side board and find the pass through connectors and see if there is voltage being applied to the heater elements when it should be heating.

Was the temperature fluctuation in the source rapid or over several hours? If rapid I would suspect a problem with the thermocouple or the circuitry that reads the temperatures from it.
The past is there to guide us into the future, not to dwell in.
It sounds very much as if you did not get a good connection when you reconnected the heater sensor. Opening up and doing it again will surely work out a lot cheaper than a new circuit board.

Peter
Peter Apps
Hi

As suggested check the thermocouple and heaters first, they do break on 5973s and can be replaced. Also check the ribbon cable that runs from the side board to the mainboard.
If the temperature is fluctuating rapidly, I would bet that it is the thermocouple is shot. I've seen it happen several times.
5 posts Page 1 of 1

Who is online

In total there is 1 user online :: 0 registered, 0 hidden and 1 guest (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: No registered users and 1 guest

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry