Advertisement

criteria for intermediate precision

Discussions about HPLC, CE, TLC, SFC, and other "liquid phase" separation techniques.

2 posts Page 1 of 1
Hi,

I want to confirm if RSD% of 12 restults (6 for each analyst) is typicaly evaluated for intermediate precision validation. This has been our practice.

Thanks.
We typically have the operator and a second analyst assay a sample five times. Each has to be within 2% RSD of their own numbers, and all 1o need to be within 3% RSD.
2 posts Page 1 of 1

Who is online

In total there are 18 users online :: 0 registered, 0 hidden and 18 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: No registered users and 18 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry