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Ethylacetoacetate

Discussions about GC and other "gas phase" separation techniques.

3 posts Page 1 of 1
Hi

why peak shape for Ethyl aceto acetate in almost all GC columns is fronting???????????
You really provided very little information.

Try more dilute injection and/or smaller injection size.
This is caused by a lack of solubility of the analyte in the liquid phase and a greater affiniity for the analyte to itself.

The 50% phenyl methyl silicone phase seems to work best.

Be glad it elutes at all.

best wishes,

Rod
3 posts Page 1 of 1

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