3-bromomethyl-3-hydroxymethyl oxetane
Posted: Wed Nov 28, 2012 2:52 pm
Hi, am trying to analyze the above compound by GC. It has been described in some patents/papers but no conditions given. Any ideas. Thanks
Care must be taken to avoid having the bromine react with solvent or column-injector surfaces.
I would inject 0.1 microliter on column onto a megabore retention gap followed by a 0.32m 624 thick film capaillary column initially, (to check for light components) then dilute the chemical in pentane and reduce the sample size until a good chromatogram is achieved.
Initial oven temperature 40C programmed at 4C/min to 200C and hold to check for late heavy components.
Flow should be about 2-3 mL per min.
FID
Good luck,
Rod