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regarding method

Posted: Thu Aug 02, 2012 2:52 pm
by rrm1987
for analysing metal complexes i.e., transition metal complexed with bromo pyridyl azo dimethyl amino phenol.but i tried HPLC method from varoius literatures.none of the method is reproduce able.Is it a right method to agead with HPLC?if it,s right method please give some suggestions to work on that.