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Alkyl lead by GC-MS

http://www.chromforum.org/viewtopic.php?t=19788

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Alkyl lead by GC-MS

Posted: Wed May 02, 2012 6:51 pm
by JonKlar
Hey guys

I've recently been tasked with creating a method for alkyl lead by GCMS. I can't seem to find any ms specific methods online and was wondering if anyone has done anything like this? If anyone does this I would be very interested in your method parameters and column of choice.

I will continue to work on this but am very greatful for any input you might have!

Thanks again,
Jon

Re: Alkyl lead by GC-MS

Posted: Wed May 02, 2012 8:04 pm
by Yama001
Our folks have done Tetraethyl and Tetramethyl lead under the EPA 8270 method.

Re: Alkyl lead by GC-MS

Posted: Wed May 02, 2012 8:25 pm
by JonKlar
Great news, thats where I planned on starting. Do you know of a vendor for reference standards?

Re: Alkyl lead by GC-MS

Posted: Thu May 03, 2012 4:15 pm
by Yama001
It looks like our BNA crew is getting them from Accustandard.

Re: Alkyl lead by GC-MS

Posted: Tue May 29, 2012 11:49 am
by mckrause
It is fall-off-a-log easy using USEPA 8260 protocol. Switch to SIM once you have conditions established and you'll have mid-ppt sensitivity.

Re: Alkyl lead by GC-MS

Posted: Thu May 31, 2012 6:37 pm
by JonKlar
This is great. Thanks so much everyone!

Jon

Re: Alkyl lead by GC-MS

Posted: Sun Jun 08, 2025 6:19 pm
by LALman
It is fall-off-a-log easy using USEPA 8260 protocol. Switch to SIM once you have conditions established and you'll have mid-ppt sensitivity.
Please give details.
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