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- Posts: 18
- Joined: Thu Jan 26, 2012 4:03 pm
recently i change the mobile gas from He to N2 and makeup gas to N2 too. I also use temperature programme for my FID splitless GC. My question is when i use N2, i set up Purge time is 0.5m,the solvent peak is good, but between solvent and decane, there are lots small peaks in there as if there is comtanmination. However, when i change gas to He and purge time still is 0.5m(purge flow is 40ml/min), i have big solvent tailing.
can you explain why?
thank you very much
