Advertisement

baseline humps, drop and noise and drop pressure

Discussions about GC and other "gas phase" separation techniques.

2 posts Page 1 of 1
Hi everybody, hope someone can help me

I am new working in GC. We have an 7890A FID detector and we do splitless injections. And now we are having problems at the baseline, but not in all the samples, a hump appears sometime first was at minute 21, then minute 28 but then without doing anything it corrected, but now it is with an alarm that doesn't reach the pressure and at the last sample run there was a baseline drop. Finally it is working but at the post run send again the alarm.
Check for a leaky septum - and then change it anyway.

Peter
Peter Apps
2 posts Page 1 of 1

Who is online

In total there are 50 users online :: 0 registered, 0 hidden and 50 guests (based on users active over the past 5 minutes)
Most users ever online was 5108 on Wed Nov 05, 2025 8:51 pm

Users browsing this forum: No registered users and 50 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry