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Resolution of Bis(2-Chloroethyl)ether and Aniline

Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.

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Resolution of Bis(2-Chloroethyl)ether and Aniline

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a2j812
Can anyone help me get resolution between Bis(2-Chloroethyl)ether and Aniline?

Re: Resolution of Bis(2-Chloroethyl)ether and Aniline

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mckrause
Yeah, it's not great. We get baseline (barely), using a 20 m x 0.18 mm 0.18 um Restek RXi-5Sil-MS, starting at 50 C. It's tricky - you need to balance your gas flows well, so that you're at optimum flow throughout the front part of the chromatogram.
Mark Krause
Laboratory Director
Krause Analytical
Austin, TX USA
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