Advertisement

OI 4660

Discussions about sample preparation: extraction, cleanup, derivatization, etc.

6 posts Page 1 of 1
Does anyone out there use OI's model 4660 concentrator for volatiles? If so, do you like it and how often do you have to change the trap?
When I used to work in the lab, I used an OI 4660 for two years and had some serious problems with a few key compounds. Never got reproducible results for two compounds. Moved to Tekmar and got much better results immediately.
I changed the trap when I lost response.

Don
Don Shelly
Don Shelly Consulting, LLC
don.shelly@donshellyconsulting.com
Chem Sam- Which key compounds did you have problems with?

Don- How often were you changing the trap?
I was trying to remember which analytes - they were heavies - I remember one being napthalene being one. I know when we changed out two of the sample pathway lines, the problem went away. But it came back within 4 months.

In regards to how often you have to change the trap - this definitely depends on how many samples you analyze. It's my understanding that most people change it ever 8 mo to a year.
*****Commercial Here******

If you choose to look at alternatives, try http://www.estanalytical.com/Products/E ... Evolution/ . We will guarantee your results and give you any help necessary.

If you are only having problems with you heavies, it could be a trap issue, but it could also be a Cyclone mgmt issue that has developed an active site. If you cannot get the help you need, feel free to call our support line at 800-283-3510. They can help you free of charge over the phone.
6 posts Page 1 of 1

Who is online

In total there are 10 users online :: 0 registered, 0 hidden and 10 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: No registered users and 10 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry