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HP5890 TCD signal going to 0 after pushing start bottom

Discussions about GC and other "gas phase" separation techniques.

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I'm using an old (~25 years old) HP5890 GC/TCD for methane gas test. Usually I wait about 30 mins for letting the signal baseline to be stable (signal will be about 50-30).
Recently, when I push the "start" bottom on the panel to start a run, the signal will go down to zero and bounce back to 30 after the run. I tried several times with calibration gas, the results are repeatable. But according to my colleague, the numbers are much lower than before.
My questions are:
(1) Is the TCD unstable? Can I use these number for quantify gas concentration?
(2) I have tried changed columns (HP-PLOTQ and CarbonPLOT), changed analytical methods, checked gas leak (N2 is the carrier gas), baked TCD. What should I try?

Thank you all in advance!
Have you tried to manually zero the detector BEFORE you start the run?

best wishes,

Rod
Yes, I tried to adjusted the base line to zero before start the run, then the signal will go down to negative values, then back to zero after the run.
Sorry if this is very obvious. Did your signal accedentally get changed to use the column compensation? If you press SIGNAL 1 (or 2) does it read A (or B) or does it include - COMP 1 (or 2)?
4 posts Page 1 of 1

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