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Sample preperation for pyradilyl

Posted: Sun Jan 16, 2011 3:18 pm
by Rachamim
Hi everybody,
(Sorry about my english this is not my native language)
I tried to figure out good method for Pyridalyl [/b ] which I want to identify via LC-MS

I have already try to add Ammonium Acetate 0.1M after the extraction (100ml/100ml v/v)for ionization but the result in 1000ppb was very poor

Any suggestion ?


Thank in advance

Re: Sample preperation for pyradilyl

Posted: Thu Mar 10, 2011 8:10 pm
by Don Shelly
Use either method AOAC 2007.01 or EN 15662.